Towards cubic modification of Li                         7                         La                         3                         Zr                         2                         O                         12                          compound by mechanical milling and annealing of powders

D. Oleszak; B. Kurowski; T. Pikula; M. Pawlyta; M. Senna; H. Suzuki

doi:10.24425/amm.2019.126211

Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders

D. Oleszak
, B. Kurowski
, T. Pikula
, M. Pawlyta
, M. Senna
, H. Suzuki

Materials Testing Laboratory (RMT/RMT L1)

Warsaw University of Technology
Lublin University of Technology
Keio University
Shizuoka University

Research output: Contribution to journal › Article › peer-review

Abstract

The aim of these studies was to obtain single phase cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ by mechanical milling and annealing of La(OH) ₃ , Li ₂ CO ₃ and ZrO ₂ powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li ₇ La ₃ Zr ₂ O ₁₂ in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

Original language	English
Pages (from-to)	13-16
Number of pages	4
Journal	Archives of Metallurgy and Materials
Volume	64
Issue number	1
DOIs	https://doi.org/10.24425/amm.2019.126211
Publication status	Published - 2019

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 7 Affordable and Clean Energy

Keywords

DSC/TG
Lithium-ion batteries
Mechanical milling
Solid state electrolyte
XRD

ASJC Scopus subject areas

Metals and Alloys

Access to Document

10.24425/amm.2019.126211

Cite this

Oleszak, D., Kurowski, B., Pikula, T., Pawlyta, M., Senna, M., & Suzuki, H. (2019). Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders Archives of Metallurgy and Materials, 64(1), 13-16. https://doi.org/10.24425/amm.2019.126211

Oleszak, D. ; Kurowski, B. ; Pikula, T. et al. / Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders In: Archives of Metallurgy and Materials. 2019 ; Vol. 64, No. 1. pp. 13-16.

@article{745eebab6c80400eac58309cdd0e7713,

title = " Towards cubic modification of Li 7 La 3 Zr 2 O 12 compound by mechanical milling and annealing of powders ",

abstract = " The aim of these studies was to obtain single phase cubic modification of Li 7 La 3 Zr 2 O 12 by mechanical milling and annealing of La(OH) 3 , Li 2 CO 3 and ZrO 2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li 7 La 3 Zr 2 O 12 in the sample structure, reaching 90\%. Thermal measurements revealed more complex reactions requiring further studies.",

keywords = "DSC/TG, Lithium-ion batteries, Mechanical milling, Solid state electrolyte, XRD",

author = "D. Oleszak and B. Kurowski and T. Pikula and M. Pawlyta and M. Senna and H. Suzuki",

year = "2019",

doi = "10.24425/amm.2019.126211",

language = "English",

volume = "64",

pages = "13--16",

journal = "Archives of Metallurgy and Materials",

issn = "1733-3490",

publisher = "Polska Akademia Nauk",

number = "1",

}

Oleszak, D, Kurowski, B, Pikula, T, Pawlyta, M, Senna, M & Suzuki, H 2019, ' Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders ', Archives of Metallurgy and Materials, vol. 64, no. 1, pp. 13-16. https://doi.org/10.24425/amm.2019.126211

Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders . / Oleszak, D.; Kurowski, B.; Pikula, T. et al.
In: Archives of Metallurgy and Materials, Vol. 64, No. 1, 2019, p. 13-16.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Towards cubic modification of Li 7 La 3 Zr 2 O 12 compound by mechanical milling and annealing of powders

AU - Oleszak, D.

AU - Kurowski, B.

AU - Pikula, T.

AU - Pawlyta, M.

AU - Senna, M.

AU - Suzuki, H.

PY - 2019

Y1 - 2019

N2 - The aim of these studies was to obtain single phase cubic modification of Li 7 La 3 Zr 2 O 12 by mechanical milling and annealing of La(OH) 3 , Li 2 CO 3 and ZrO 2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li 7 La 3 Zr 2 O 12 in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

AB - The aim of these studies was to obtain single phase cubic modification of Li 7 La 3 Zr 2 O 12 by mechanical milling and annealing of La(OH) 3 , Li 2 CO 3 and ZrO 2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li 7 La 3 Zr 2 O 12 in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

KW - DSC/TG

KW - Lithium-ion batteries

KW - Mechanical milling

KW - Solid state electrolyte

KW - XRD

UR - https://www.scopus.com/pages/publications/85063722965

U2 - 10.24425/amm.2019.126211

DO - 10.24425/amm.2019.126211

M3 - Article

AN - SCOPUS:85063722965

SN - 1733-3490

VL - 64

SP - 13

EP - 16

JO - Archives of Metallurgy and Materials

JF - Archives of Metallurgy and Materials

IS - 1

ER -

Oleszak D, Kurowski B, Pikula T, Pawlyta M, Senna M, Suzuki H. Towards cubic modification of Li ₇ La ₃ Zr ₂ O ₁₂ compound by mechanical milling and annealing of powders Archives of Metallurgy and Materials. 2019;64(1):13-16. doi: 10.24425/amm.2019.126211