Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions

Alicja Kazek-Kȩsik; Grzegorz Dercz; Izabela Kalemba; Katarzyna Suchanek; Andrey I. Kukharenko; Danila M. Korotin; Joanna Michalska; Agnieszka Krza̧kała; Jerzy Piotrowski; Ernst Z. Kurmaev; Seif O. Cholakh; Wojciech Simka

doi:10.1016/j.msec.2014.03.008

Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions

Alicja Kazek-Kȩsik
, Grzegorz Dercz
, Izabela Kalemba
, Katarzyna Suchanek
, Andrey I. Kukharenko
, Danila M. Korotin
, Joanna Michalska
, Agnieszka Krza̧kała
, Jerzy Piotrowski
, Ernst Z. Kurmaev
, Seif O. Cholakh
, Wojciech Simka

Department of Inorganic Chemistry, Analytical Chemistry and Electrochemistry (RCH/RCH1)

University of Silesia in Katowice
AGH University of Krakow
Institute of Nuclear Physics PAN
Institute of Metal Physics, Russian Academy of Sciences-Ural Division
Ural Federal University
Silesian University of Technology

Research output: Contribution to journal › Article › peer-review

33 Citations (Scopus)

Abstract

This paper reports on the surface modification of a Ti-15Mo alloy by plasma electrolytic oxidation (PEO). This process was carried out in solutions of 0.1 M Ca(H₂PO₂)₂ with various concentrations of tricalcium phosphate (Ca₃(PO₄)₂), wollastonite (CaSiO₃), or silica (SiO₂) using voltages of up to 350 V. The surface microstructure (SEM, cross-section of coating), roughness and chemical composition (energy-dispersive X-ray spectroscopy, thin layer X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy) of the porous oxide layers were investigated. The concentration of powder added to the solution changed the chemical composition and morphology of PEO coatings on the Ti-15Mo alloy surface. Calcium and phosphorous compounds were detected in the coatings formed on the substrate by the PEO process at 300 V.

Original language	English
Pages (from-to)	259-272
Number of pages	14
Journal	Materials Science and Engineering C
Volume	39
Issue number	1
DOIs	https://doi.org/10.1016/j.msec.2014.03.008
Publication status	Published - 1 Jun 2014

Keywords

Plasma electrolytic oxidation
Silica
Surface modification
TCP
Vanadium-free titanium alloy
Wollastonite

ASJC Scopus subject areas

General Medicine

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10.1016/j.msec.2014.03.008

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Kazek-Kȩsik, A., Dercz, G., Kalemba, I., Suchanek, K., Kukharenko, A. I., Korotin, D. M., Michalska, J., Krza̧kała, A., Piotrowski, J., Kurmaev, E. Z., Cholakh, S. O., & Simka, W. (2014). Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions. Materials Science and Engineering C, 39(1), 259-272. https://doi.org/10.1016/j.msec.2014.03.008

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title = "Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions",

abstract = "This paper reports on the surface modification of a Ti-15Mo alloy by plasma electrolytic oxidation (PEO). This process was carried out in solutions of 0.1 M Ca(H2PO2)2 with various concentrations of tricalcium phosphate (Ca3(PO4)2), wollastonite (CaSiO3), or silica (SiO2) using voltages of up to 350 V. The surface microstructure (SEM, cross-section of coating), roughness and chemical composition (energy-dispersive X-ray spectroscopy, thin layer X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy) of the porous oxide layers were investigated. The concentration of powder added to the solution changed the chemical composition and morphology of PEO coatings on the Ti-15Mo alloy surface. Calcium and phosphorous compounds were detected in the coatings formed on the substrate by the PEO process at 300 V.",

keywords = "Plasma electrolytic oxidation, Silica, Surface modification, TCP, Vanadium-free titanium alloy, Wollastonite",

author = "Alicja Kazek-Kȩsik and Grzegorz Dercz and Izabela Kalemba and Katarzyna Suchanek and Kukharenko, \{Andrey I.\} and Korotin, \{Danila M.\} and Joanna Michalska and Agnieszka Krz{\c a}ka{\l}a and Jerzy Piotrowski and Kurmaev, \{Ernst Z.\} and Cholakh, \{Seif O.\} and Wojciech Simka",

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Kazek-Kȩsik, A, Dercz, G, Kalemba, I, Suchanek, K, Kukharenko, AI, Korotin, DM, Michalska, J, Krza̧kała, A, Piotrowski, J, Kurmaev, EZ, Cholakh, SO & Simka, W 2014, 'Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions', Materials Science and Engineering C, vol. 39, no. 1, pp. 259-272. https://doi.org/10.1016/j.msec.2014.03.008

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T1 - Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions

AU - Kazek-Kȩsik, Alicja

AU - Dercz, Grzegorz

AU - Kalemba, Izabela

AU - Suchanek, Katarzyna

AU - Kukharenko, Andrey I.

AU - Korotin, Danila M.

AU - Michalska, Joanna

AU - Krza̧kała, Agnieszka

AU - Piotrowski, Jerzy

AU - Kurmaev, Ernst Z.

AU - Cholakh, Seif O.

AU - Simka, Wojciech

PY - 2014/6/1

Y1 - 2014/6/1

N2 - This paper reports on the surface modification of a Ti-15Mo alloy by plasma electrolytic oxidation (PEO). This process was carried out in solutions of 0.1 M Ca(H2PO2)2 with various concentrations of tricalcium phosphate (Ca3(PO4)2), wollastonite (CaSiO3), or silica (SiO2) using voltages of up to 350 V. The surface microstructure (SEM, cross-section of coating), roughness and chemical composition (energy-dispersive X-ray spectroscopy, thin layer X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy) of the porous oxide layers were investigated. The concentration of powder added to the solution changed the chemical composition and morphology of PEO coatings on the Ti-15Mo alloy surface. Calcium and phosphorous compounds were detected in the coatings formed on the substrate by the PEO process at 300 V.

AB - This paper reports on the surface modification of a Ti-15Mo alloy by plasma electrolytic oxidation (PEO). This process was carried out in solutions of 0.1 M Ca(H2PO2)2 with various concentrations of tricalcium phosphate (Ca3(PO4)2), wollastonite (CaSiO3), or silica (SiO2) using voltages of up to 350 V. The surface microstructure (SEM, cross-section of coating), roughness and chemical composition (energy-dispersive X-ray spectroscopy, thin layer X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy) of the porous oxide layers were investigated. The concentration of powder added to the solution changed the chemical composition and morphology of PEO coatings on the Ti-15Mo alloy surface. Calcium and phosphorous compounds were detected in the coatings formed on the substrate by the PEO process at 300 V.

KW - Plasma electrolytic oxidation

KW - Silica

KW - Surface modification

KW - TCP

KW - Vanadium-free titanium alloy

KW - Wollastonite

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DO - 10.1016/j.msec.2014.03.008

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AN - SCOPUS:84897827617

SN - 0928-4931

VL - 39

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EP - 272

JO - Materials Science and Engineering C

JF - Materials Science and Engineering C

IS - 1

ER -

Surface characterisation of Ti-15Mo alloy modified by a PEO process in various suspensions

Abstract

Keywords

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