Sonochemical preparation of SbSI gel

M. Nowak; P. Szperlich; Bober; J. Szala; G. Moskal; D. Stróz

doi:10.1016/j.ultsonch.2007.09.003

Sonochemical preparation of SbSI gel

M. Nowak
, P. Szperlich
, Bober
, J. Szala
, G. Moskal
, D. Stróz

Silesian University of Technology
University of Silesia in Katowice

Research output: Contribution to journal › Article › peer-review

82 Citations (Scopus)

Abstract

A novel sonochemical method for direct preparation of nanocrystalline antimony sulfoiodide (SbSI) has been established. The SbSI gel was synthesized using elemental Sb, S and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm²) at 50 °C for 2 h. The products were characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with diameters of about 10-50 nm and lengths reaching up to several micrometers and single-crystalline in nature.

Original language	English
Pages (from-to)	709-716
Number of pages	8
Journal	Ultrasonics Sonochemistry
Volume	15
Issue number	5
DOIs	https://doi.org/10.1016/j.ultsonch.2007.09.003
Publication status	Published - Jul 2008

Keywords

Antimony sulfoiodide
Ferroelectric materials
Nanocrystals
Sonochemistry

ASJC Scopus subject areas

Chemical Engineering (miscellaneous)
Environmental Chemistry
Radiology, Nuclear Medicine and Imaging
Acoustics and Ultrasonics
Organic Chemistry
Inorganic Chemistry

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10.1016/j.ultsonch.2007.09.003

Cite this

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title = "Sonochemical preparation of SbSI gel",

abstract = "A novel sonochemical method for direct preparation of nanocrystalline antimony sulfoiodide (SbSI) has been established. The SbSI gel was synthesized using elemental Sb, S and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The products were characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with diameters of about 10-50 nm and lengths reaching up to several micrometers and single-crystalline in nature.",

keywords = "Antimony sulfoiodide, Ferroelectric materials, Nanocrystals, Sonochemistry",

author = "M. Nowak and P. Szperlich and Bober and J. Szala and G. Moskal and D. Str{\'o}z",

year = "2008",

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doi = "10.1016/j.ultsonch.2007.09.003",

language = "English",

volume = "15",

pages = "709--716",

journal = "Ultrasonics Sonochemistry",

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TY - JOUR

T1 - Sonochemical preparation of SbSI gel

AU - Nowak, M.

AU - Szperlich, P.

AU - Bober,

AU - Szala, J.

AU - Moskal, G.

AU - Stróz, D.

PY - 2008/7

Y1 - 2008/7

N2 - A novel sonochemical method for direct preparation of nanocrystalline antimony sulfoiodide (SbSI) has been established. The SbSI gel was synthesized using elemental Sb, S and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The products were characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with diameters of about 10-50 nm and lengths reaching up to several micrometers and single-crystalline in nature.

AB - A novel sonochemical method for direct preparation of nanocrystalline antimony sulfoiodide (SbSI) has been established. The SbSI gel was synthesized using elemental Sb, S and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The products were characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with diameters of about 10-50 nm and lengths reaching up to several micrometers and single-crystalline in nature.

KW - Antimony sulfoiodide

KW - Ferroelectric materials

KW - Nanocrystals

KW - Sonochemistry

UR - https://www.scopus.com/pages/publications/41549136444

U2 - 10.1016/j.ultsonch.2007.09.003

DO - 10.1016/j.ultsonch.2007.09.003

M3 - Article

AN - SCOPUS:41549136444

SN - 1350-4177

VL - 15

SP - 709

EP - 716

JO - Ultrasonics Sonochemistry

JF - Ultrasonics Sonochemistry

IS - 5

ER -

Sonochemical preparation of SbSI gel

Abstract

Keywords

ASJC Scopus subject areas

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