Sonochemical preparation of SbSeI gel

M. Nowak; B. Kauch; P. Szperlich; M. Jesionek; M. Kepińska; Bober; J. Szala; G. Moskal; T. Rzychoń; D. Stróz

doi:10.1016/j.ultsonch.2009.01.003

Sonochemical preparation of SbSeI gel

M. Nowak
, B. Kauch
, P. Szperlich
, M. Jesionek
, M. Kepińska
, Bober
, J. Szala
, G. Moskal
, T. Rzychoń
, D. Stróz

Warsaw University of Life Sciences
Silesian University of Technology
University of Silesia in Katowice

Research output: Contribution to journal › Article › peer-review

26 Citations (Scopus)

Abstract

A novel sonochemical method for direct preparation of nanocrystalline antimony selenoiodide (SbSeI) has been established. The SbSeI gel was synthesized using elemental Sb, Se, and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm²) at 50 °C for 2 h. The product was characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with lateral dimensions of about 20-50 nm and lengths reaching up to several micrometers and single crystalline in nature.

Original language	English
Pages (from-to)	546-551
Number of pages	6
Journal	Ultrasonics Sonochemistry
Volume	16
Issue number	4
DOIs	https://doi.org/10.1016/j.ultsonch.2009.01.003
Publication status	Published - Apr 2009

Keywords

Antimony selenoiodide
Nanocrystals
Sonochemistry

ASJC Scopus subject areas

Chemical Engineering (miscellaneous)
Environmental Chemistry
Radiology, Nuclear Medicine and Imaging
Acoustics and Ultrasonics
Organic Chemistry
Inorganic Chemistry

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10.1016/j.ultsonch.2009.01.003

Cite this

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title = "Sonochemical preparation of SbSeI gel",

abstract = "A novel sonochemical method for direct preparation of nanocrystalline antimony selenoiodide (SbSeI) has been established. The SbSeI gel was synthesized using elemental Sb, Se, and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The product was characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with lateral dimensions of about 20-50 nm and lengths reaching up to several micrometers and single crystalline in nature.",

keywords = "Antimony selenoiodide, Nanocrystals, Sonochemistry",

author = "M. Nowak and B. Kauch and P. Szperlich and M. Jesionek and M. Kepi{\'n}ska and Bober and J. Szala and G. Moskal and T. Rzycho{\'n} and D. Str{\'o}z",

year = "2009",

month = apr,

doi = "10.1016/j.ultsonch.2009.01.003",

language = "English",

volume = "16",

pages = "546--551",

journal = "Ultrasonics Sonochemistry",

issn = "1350-4177",

publisher = "Elsevier B.V.",

number = "4",

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TY - JOUR

T1 - Sonochemical preparation of SbSeI gel

AU - Nowak, M.

AU - Kauch, B.

AU - Szperlich, P.

AU - Jesionek, M.

AU - Kepińska, M.

AU - Bober,

AU - Szala, J.

AU - Moskal, G.

AU - Rzychoń, T.

AU - Stróz, D.

PY - 2009/4

Y1 - 2009/4

N2 - A novel sonochemical method for direct preparation of nanocrystalline antimony selenoiodide (SbSeI) has been established. The SbSeI gel was synthesized using elemental Sb, Se, and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The product was characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with lateral dimensions of about 20-50 nm and lengths reaching up to several micrometers and single crystalline in nature.

AB - A novel sonochemical method for direct preparation of nanocrystalline antimony selenoiodide (SbSeI) has been established. The SbSeI gel was synthesized using elemental Sb, Se, and I in the presence of ethanol under ultrasonic irradiation (35 kHz, 2 W/cm2) at 50 °C for 2 h. The product was characterized by using techniques such as powder X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED), and optical diffuse reflection spectroscopy (DRS). The SEM and HRTEM investigations exhibit that the as-prepared samples are made up of large quantity nanowires with lateral dimensions of about 20-50 nm and lengths reaching up to several micrometers and single crystalline in nature.

KW - Antimony selenoiodide

KW - Nanocrystals

KW - Sonochemistry

UR - https://www.scopus.com/pages/publications/60949093890

U2 - 10.1016/j.ultsonch.2009.01.003

DO - 10.1016/j.ultsonch.2009.01.003

M3 - Article

C2 - 19217339

AN - SCOPUS:60949093890

SN - 1350-4177

VL - 16

SP - 546

EP - 551

JO - Ultrasonics Sonochemistry

JF - Ultrasonics Sonochemistry

IS - 4

ER -

Sonochemical preparation of SbSeI gel

Abstract

Keywords

ASJC Scopus subject areas

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