Ocena procesu utwardzania bezformaldehydowej żywicy melaminowej z wykorzystaniem analizy termicznej i spektroskopii w podczerwieni

Justyna Chrobak; Ewa Sabura; Jolanta Iłowska; Anna Chrobok

doi:10.15199/62.2024.9.14

Ocena procesu utwardzania bezformaldehydowej żywicy melaminowej z wykorzystaniem analizy termicznej i spektroskopii w podczerwieni

Translated title of the contribution: The evaluation of curing process of formaldehyde-free melamine resin using thermal analysis and infrared spectroscopy

Justyna Chrobak
, Ewa Sabura
, Jolanta Iłowska
, Anna Chrobok

Department of Chemical Organic Technology and Petrochemistry (RCH/RCH5)

Institute of Heavy Organic Synthesis "Blachownia"
Silesian University of Technology

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

Melamine-glyoxal-glycerin (MG) and melamine-glyoxal-HCHO-glycerin resins were synthesized, in which 10, 20 and 30% by mass of glyoxal was replaced by HCHO. Thermal analysis (TGA and DSC) and IR spectroscopy were used to evaluate the curing process using urea-NH4NO3 soln. The effect of adding a variable amt. of HCHO on the parameters of the curing process was detd. MG resins could be of both chem. curing, using a hardener, and thermal curing at 120°C.

Translated title of the contribution	The evaluation of curing process of formaldehyde-free melamine resin using thermal analysis and infrared spectroscopy
Original language	Polish
Pages (from-to)	1029-1033
Number of pages	5
Journal	Przemysl Chemiczny
Volume	103
Issue number	9
DOIs	https://doi.org/10.15199/62.2024.9.14
Publication status	Published - 2024

ASJC Scopus subject areas

General Chemistry
General Chemical Engineering

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title = "Ocena procesu utwardzania bezformaldehydowej {\.z}ywicy melaminowej z wykorzystaniem analizy termicznej i spektroskopii w podczerwieni",

abstract = "Melamine-glyoxal-glycerin (MG) and melamine-glyoxal-HCHO-glycerin resins were synthesized, in which 10, 20 and 30\% by mass of glyoxal was replaced by HCHO. Thermal analysis (TGA and DSC) and IR spectroscopy were used to evaluate the curing process using urea-NH4NO3 soln. The effect of adding a variable amt. of HCHO on the parameters of the curing process was detd. MG resins could be of both chem. curing, using a hardener, and thermal curing at 120°C.",

keywords = "DSC, IR, TGA, curing, formaldehyde-free amine resins",

author = "Justyna Chrobak and Ewa Sabura and Jolanta I{\l}owska and Anna Chrobok",

year = "2024",

doi = "10.15199/62.2024.9.14",

language = "polski",

volume = "103",

pages = "1029--1033",

journal = "Przemysl Chemiczny",

issn = "0033-2496",

publisher = "Wydawnictwo SIGMA - N O T Sp. z o.o.",

number = "9",

}

TY - JOUR

T1 - Ocena procesu utwardzania bezformaldehydowej żywicy melaminowej z wykorzystaniem analizy termicznej i spektroskopii w podczerwieni

AU - Chrobak, Justyna

AU - Sabura, Ewa

AU - Iłowska, Jolanta

AU - Chrobok, Anna

PY - 2024

Y1 - 2024

N2 - Melamine-glyoxal-glycerin (MG) and melamine-glyoxal-HCHO-glycerin resins were synthesized, in which 10, 20 and 30% by mass of glyoxal was replaced by HCHO. Thermal analysis (TGA and DSC) and IR spectroscopy were used to evaluate the curing process using urea-NH4NO3 soln. The effect of adding a variable amt. of HCHO on the parameters of the curing process was detd. MG resins could be of both chem. curing, using a hardener, and thermal curing at 120°C.

AB - Melamine-glyoxal-glycerin (MG) and melamine-glyoxal-HCHO-glycerin resins were synthesized, in which 10, 20 and 30% by mass of glyoxal was replaced by HCHO. Thermal analysis (TGA and DSC) and IR spectroscopy were used to evaluate the curing process using urea-NH4NO3 soln. The effect of adding a variable amt. of HCHO on the parameters of the curing process was detd. MG resins could be of both chem. curing, using a hardener, and thermal curing at 120°C.

KW - DSC

KW - IR

KW - TGA

KW - curing

KW - formaldehyde-free amine resins

UR - https://www.scopus.com/pages/publications/85213400762

U2 - 10.15199/62.2024.9.14

DO - 10.15199/62.2024.9.14

M3 - Artykuł

AN - SCOPUS:85213400762

SN - 0033-2496

VL - 103

SP - 1029

EP - 1033

JO - Przemysl Chemiczny

JF - Przemysl Chemiczny

IS - 9

ER -

Ocena procesu utwardzania bezformaldehydowej żywicy melaminowej z wykorzystaniem analizy termicznej i spektroskopii w podczerwieni

Abstract

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